HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylhydrazine → HCID 19025425, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylhydrazine | HCID 6061 | — |
| Reactant | Benzonitrile, 4-isothiocyanato- | HCID 17626 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19025425 | HCID 19025425 | 98.9% |
Reaction Steps
Following procedures similar to those employed in Step A of Example 2, the reaction of 7.8 g (0.049 mole) of 4-cyanophenyl isothiocyanate with 2.24 g (0.0490 mole) of methylhydrazine in 50 ml of ethanol yielded 10.0 g of 4-(4-cyanophenyl)-2-methyl-3-thiosemicarbazide as a solid, mp 178°-179° C. The nmr spectrum was consistent with the proposed structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05108486 |
| Source dataset | uspto-grants-1992_04 |
| ORD ID | ord-2b1e9750f5d04a50845ae24d150a009e |
| Source note | uspto-grants-1992_04 |