HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15617368, compound → HCID 15617270, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15617368 | HCID 15617368 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 15617270 | HCID 15617270 | 92% |
Reaction Steps
A solution of 2.58 g of 3-acetoxymethyl-2-carboethoxy-N-(1,1-dimethylethyl)benzenesulfonamide in 25 mL of trifluoroacetic acid was stirred at room temperature overnight. Removal of the solvent on the rotovap followed by trituration with n-butyl chloride provided 2.0 g of a white solid, m.p. 98°-100° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05108487 |
| Source dataset | uspto-grants-1992_04 |
| ORD ID | ord-47c19e9de3854fa7b486d5dbee6286cc |
| Source note | uspto-grants-1992_04 |