HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → 1-Propyl-4-p-propylphenylcyclohexan-1-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | 4-(4-Propylphenyl)cyclohexan-1-one | HCID 14495754 | — |
| Reactant | 1-Propyl-4-p-propylphenylcyclohexene | HCID 19819364 | — |
| Reactant | HCID 178455851 | HCID 178455851 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 1-Propyl-4-p-propylphenylcyclohexan-1-ol | HCID 19819403 | — |
Reaction Steps
HBr is passed, at 0°, into a solution in 50 ml of CH2Cl2 of 2.42 g of 1-propyl-4-p-propylphenylcyclohexene (obtainable by reacting 4-p-propylphenylcyclohexanone with C3H7MgBr, hydrolysing the product to give 1-propyl-4-p-propylphenylcyclohexan-1-ol and dehydrating the latter), the mixture is allowed to stand overnight and is worked up in the customary manner to give r-1-bromo-1-propyl-cis-4-p-propylphenylcyclohexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05108652 |
| Source dataset | uspto-grants-1992_04 |
| ORD ID | ord-95b87b91357a4625bde7a9996908c384 |
| Source note | uspto-grants-1992_04 |