1-Chloro-5-hydroxy-5-methylhexane → 7-Allyl-3-ethyl-1-(5-hydroxy-5-methylhexyl)-xanthine

HRID 1031079Notes

Reaction equation

HRID 1031079 reaction equation
[CH2:1]([N:4]1[C:12]2[C:11](=[O:13])[NH:10][C:9](=[O:14])[N:8]([CH2:15][CH3:16])[C:7]=2[N:6]=[CH:5]1)[CH:2]=[CH2:3].Cl[CH2:18][CH2:19][CH2:20][CH2:21][C:22]([OH:25])([CH3:24])[CH3:23]>>[CH2:1]([N:4]1[C:12]2[C:11](=[O:13])[N:10]([CH2:18][CH2:19][CH2:20][CH2:21][C:22]([OH:25])([CH3:24])[CH3:23])[C:9](=[O:14])[N:8]([CH2:15][CH3:16])[C:7]=2[N:6]=[CH:5]1)[CH:2]=[CH2:3]

Participants

3

Reactant 2

HCID 137476791-Chloro-5-hydroxy-5-methylhexaneHCID 19819649HCID 19819649, compound

Product 1

HCID 198196457-Allyl-3-ethyl-1-(5-hydroxy-5-methylhexyl)-xanthine

Procedure

This compound was prepared as described in Example 1 starting with 7-Allyl-3-ethyl-xanthine and 1-chloro-5-hydroxy-5-methylhexane and recrystallizing the final product from diisopropyl ether with addition of some ethyl acetate.

Workup

  1. customThis compound was prepared
  2. customrecrystallizing the final product from diisopropyl ether
  3. additionwith addition of some ethyl acetate

Sources & evidence

ORD record
ord-d1516ff5bef24b61b100c1118fef7ec1
Source dataset
uspto-grants-1992_04
Patent number
US05109003

Reaction notes

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