HuagongsheHuagongshe Chemistry Print Report · For research reference only
[2,6-Dichloro-4-(trifluoromethyl)phenyl]hydrazine → HCID 136403371, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | [2,6-Dichloro-4-(trifluoromethyl)phenyl]hydrazine | HCID 688223 | — |
| Reactant | HCID 71434845 | HCID 71434845 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 136403371 | HCID 136403371 | — |
Reaction Steps
2,6-Dichloro-4-trifluoromethylphenylhydrazine (6.6 g) and 1-hexene-4,5-dione 4-oxime (3.4 g) were stirred in diethyl ether (200 ml) for 18 hours. The solvent was removed under reduced pressure to give 1-hexene-4,5-dione 5-(2,6-dichloro-4-trifluoromethylphenylhydrazone) 4-oxime, m.p. 86°-88°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05109012 |
| Source dataset | uspto-grants-1992_04 |
| ORD ID | ord-4ec84d9473e04a1f9f1856070ae1cf41 |
| Source note | uspto-grants-1992_04 |