Methyl vinyl ketone → HCID 19698840, compound

HRID 1031218Notes

Reaction equation

HRID 1031218 reaction equation
[C:1]1([CH2:7][NH:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][NH:16][CH2:17][C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH:24]([C:26]([CH3:28])=[O:27])=[CH2:25]>CO>[O:27]=[C:26]([CH3:28])[CH2:24][CH2:25][N:16]([CH2:17][C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1)[CH2:15][CH2:14][CH2:13][CH2:12][CH2:11][CH2:10][CH2:9][N:8]([CH2:25][CH2:24][C:26](=[O:27])[CH3:28])[CH2:7][C:1]1[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

Participants

4

Reactant 2

HCID 6570Methyl vinyl ketoneHCID 14856215HCID 14856215, compound

Product 1

HCID 19698840HCID 19698840, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Dissolve N,N'-bis[(phenyl)methyl]-1,7-heptanediamine (9.3 g, 0.03 mol) in methanol (120 ml) and while stirring the mixture introduce methyl vinyl ketone (5.6 ml, 0.066 mol) in a stream of nitrogen gas. Stir the mixture for 18 hours to yield the title compound.

Workup

  1. stirringStir the mixture for 18 hours

Sources & evidence

ORD record
ord-2e2f029038f442d5bc42ad87d25ee951
Source dataset
uspto-grants-1992_04
Patent number
US05109024

Reaction notes

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