HCID 10497335, compound → HCID 14155093, compound

HRID 1031353Notes

Reaction equation

HRID 1031353 reaction equation
[CH2:1]([S:8][C:9]1[N:23]=[C:12]2[N:13]=[C:14]([O:17][CH2:18][C:19](F)(F)F)[CH:15]=[CH:16][N:11]2[N:10]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1>C(O)C>[CH2:1]([S:8][C:9]1[N:23]=[C:12]2[N:13]=[C:14]([O:17][CH2:18][CH3:19])[CH:15]=[CH:16][N:11]2[N:10]=1)[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 1

HCID 10497335HCID 10497335, compound

Product 1

HCID 14155093HCID 14155093, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

This material was prepared by heating 2-benzylthio-5-(2,2,2-trifluoroethoxy)-1,2,4-triazolo[1,5-a]-pyrimidine in boiling ethanol. The hot mixture was filtered and the filtrate was concentrated. The crude product was recrystallized from isopropanol to yield the desired product as a solid, m.p. 115°-117° C. IR and 1H NMR spectra were in agreement with the assigned structure.

Workup

  1. customThis material was prepared
  2. filtrationThe hot mixture was filtered
  3. concentrationthe filtrate was concentrated
  4. customThe crude product was recrystallized from isopropanol

Sources & evidence

ORD record
ord-7cf38a08a30a4011b13d66b9c18bec4a
Source dataset
uspto-grants-1990_09
Patent number
US04954163

Reaction notes

Loading…