HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Disulfide → 2-Fluoro-6-(methylsulfanyl)aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Disulfide | HCID 12232 | — |
| Reactant | Tert-butyl 2-fluorophenylcarbamate | HCID 4935500 | — |
| Product | 2-Fluoro-6-(methylsulfanyl)aniline | HCID 11768825 | — |
Reaction Steps
This material was prepared for N-t-butoxycarbonyl-2-fluoroaniline and dimethyl disulfide following the general procedure outlined in Example 102. IR and 1H NMR spectra of the product were consistent with the assigned structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04954163 |
| Source dataset | uspto-grants-1990_09 |
| ORD ID | ord-95a28071e8b44b01aab444210662c82d |
| Source note | uspto-grants-1990_09 |