HCID 22167633, compound → HCID 22167635, compound

Participants

Reaction Steps

1-Dimethylamino-9-pentyl-8-tetradecene (Example 26c) (7.5 g) was hydrogenated in ethanol (75 ml) at 45 psi in the presence of 10% Pd/C (0.7 g) at room temperature for 5 hours. The reaction mixture was filtered and evaporated to dryness. The resulting oil was purified by distillation at 0 01 torr (in a Kugelrohr apparatus at 210°) to give 1-dimethylamino-9-pentyltetradecane as a colourless oil (5.7 g, 76%).

Provenance & Evidence