HuagongsheHuagongshe Chemistry Print Report · For research reference only
1H-indole-2-carbonyl Chloride → HCID 19896780, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1H-indole-2-carbonyl Chloride | HCID 11816208 | — |
| Reactant | HCID 19896766 | HCID 19896766 | — |
| Product | HCID 19896780 | HCID 19896780 | 45% |
Reaction Steps
In a manner analogous to that described in Example 2, from indole-2-carboxylic acid chloride and 4,4-dimethyl-6,7-diamino-1,2,3,4-tetrahydroquinolin-2one (see Example 13 a)), after column chromatography, there was obtained a yield of 45% of theory of the title compound; m.p. 264 -267° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04954498 |
| Source dataset | uspto-grants-1990_09 |
| ORD ID | ord-7238b17b1715493e9ca884f5d955c965 |
| Source note | uspto-grants-1990_09 |