HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Propanediamine → HCID 14459478, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Propanediamine | HCID 428 | — |
| Reactant | HCID 14459457 | HCID 14459457 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 14459478 | HCID 14459478 | — |
Reaction Steps
14.0 g (50 mmol) of 6-(4-chloro-3-nitro-phenyl)-4,5-dihydro-5-hydroxymethyl-3(2H)-pyridazinone are heated to 60° C. together with 50 ml of 1,3-diaminopropane in 40 ml of dioxane for 8 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04954501 |
| Source dataset | uspto-grants-1990_09 |
| ORD ID | ord-1d536c62880c489b90cf0de79f635bca |
| Source note | uspto-grants-1990_09 |