HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 22168034, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Dicyclohexylcarbodiimide | HCID 10868 | — |
| Reactant | 3,4-Dichlorophenylacetic acid | HCID 79874 | — |
| Reactant | HCID 22168074 | HCID 22168074 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 22168034 | HCID 22168034 | — |
Reaction Steps
Prepared as Ex. No. 5, from 6 g (15.23 mmoles) of 1-(pyrrolidin-1-yl)methyl-6-hydroxy-1,2,3,4-tetrahydroisoquinoline dihydrobromide, 4.1 g (20.0 mmoles) of 3,4-dichlorophenylacetic acid, 5.4 ml (38.42 mmoles) of triethylamine and 6.2 g (30.24 mmoles) of dicyclohexylcarbodiimide in 145 ml of dry chloroform.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04954509 |
| Source dataset | uspto-grants-1990_09 |
| ORD ID | ord-8892e40aa4cf416eba83881cc83692fd |
| Source note | uspto-grants-1990_09 |