HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(4-(Trifluoromethyl)phenyl)acetyl chloride → HCID 67869678, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(4-(Trifluoromethyl)phenyl)acetyl chloride | HCID 14810943 | — |
| Reactant | HCID 15005443 | HCID 15005443 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 67869678 | HCID 67869678 | — |
Reaction Steps
750 mg (3.05 mmoles) of 1-(pyrrolidin-1-yl)methyl-5-methoxy1,2,3,4-tetrahydroisoquinoline were dissolved in 10 ml of dry chloroform. 810 mg (3.64 mmoles) of 4-trifluoromethylphenyl acetyl chloride, dissolved in 10 ml of chloroform, were added dropwise to the solution at 0° C. The reaction mixture was allowed to reach room temperature and left overnight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04954509 |
| Source dataset | uspto-grants-1990_09 |
| ORD ID | ord-01a2b100850643bdaf46a81f8d388d3a |
| Source note | uspto-grants-1990_09 |