HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 3-cyano-7-methylsulfonylamino-6-phenoxy-4H-1-benzopyran-4-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 3-carbamoyl-7-methylsulfonylamino-6-phenoxy-4H-1-benzopyran-4-one | HCID 10785596 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 3-cyano-7-methylsulfonylamino-6-phenoxy-4H-1-benzopyran-4-one | HCID 14722415 | — |
Reaction Steps
3-Carbamoyl-7-methylsulfonylamino-6-phenoxy-4H-1-benzopyran-4-one was reacted with thionyl chloride in N,N-dimethylformamide to obtain 3-cyano-7-methylsulfonylamino-6-phenoxy-4H-1-benzopyran-4-one. The properties (melting point and IR) of this compound were identical with those of the compound obtained in Example 4.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04954518 |
| Source dataset | uspto-grants-1990_09 |
| ORD ID | ord-6ab6da674f054e4c8e09f5ff83724807 |
| Source note | uspto-grants-1990_09 |