HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Dioxane hydrochloride → HCID 13689669, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Reactant | HCID 178453621 | HCID 178453621 | — |
| Product | HCID 13689669 | HCID 13689669 | — |
Reaction Steps
To the compound (I) (2.00 g), 4N hydrogen chloride/1,4-dioxane solution (36 ml) was added, and the mixture was stirred under room temperature for one hour. The solvent was evaporated under a reduced pressure and toluene was added to the residue, followed by reevaporation to give L-phenylalanine methylamide hydrochloride quantitatively as a white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04954512 |
| Source dataset | uspto-grants-1990_09 |
| ORD ID | ord-25d45ab4575f448893b75d75b5648a25 |
| Source note | uspto-grants-1990_09 |