Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | HCID 14670763 | HCID 14670763 | — |
| Product | HCID 14670764 | HCID 14670764 | — |
Reaction Steps
248 g of the 1,2-bistrifluoromethoxybenzene thus obtained were allowed to drop at 0° C. in the course of 2 hours into 250 g of a mixture of 33% by weight of nitric acid and 67% by weight of sulphuric acid. The mixture was subsequently stirred at 0° C. for 5 hours, then added to ice water, and the organic phase was separated off and distilled. 284 g of 99% strength 3,4-bistrifluoromethoxynitrobenzene were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04956370 |
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| Source dataset | uspto-grants-1990_09 |
|---|
| ORD ID | ord-2c38ed83fd6748fba8f4568fbcec3c0c |
|---|
| Source note | uspto-grants-1990_09 |
|---|
