HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonyl chloride → HCID 14988477, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | HCID 15106991 | HCID 15106991 | — |
| Product | HCID 14988477 | HCID 14988477 | 79.9% |
Reaction Steps
The title compound was prepared (79.9% yield) from methyl 6-amino-1,2,3,4-tetrahydroquinoline-8-carboxylate by the same procedure as in Example 32 by using methanesulfonyl chloride instead of p-toluenesulfonyl chloride. This compound was recrystallized form ethanol to give yellow crystals, mp 244° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04956372 |
| Source dataset | uspto-grants-1990_09 |
| ORD ID | ord-60e4b264a6f640958f22fb3a999512e8 |
| Source note | uspto-grants-1990_09 |