HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1032210Generated: October 25, 2026
Dimethyl acetylenedicarboxylate → HCID 178498586, compound
https://huagongshe.com/reaction/1032210
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dimethyl acetylenedicarboxylate | HCID 12980 | — |
| Reactant | (5-amino-1H-1,2,4-triazol-3-yl)methanol | HCID 222697 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178498586 | HCID 178498586 | — |
Reaction Steps
In 1.7 liters of methanol was suspended 60 g of 3-amino-5-hydroxymethyl-1,2,4-triazole and 75 ml of dimethyl acetylenedicarboxylate was added to the suspension, and the mixture was stirred at 30° C. for 20 hours. Precipitates were collected by filtration, washed with methanol and then dried to obtain 25.7 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04956462 |
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| Source dataset | uspto-grants-1990_09 |
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| ORD ID | ord-d9c5e135ca3b46f8aeeb36751ae36b39 |
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| Source note | uspto-grants-1990_09 |
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