HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22165562, compound → HCID 53928314, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22165562 | HCID 22165562 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 53928314 | HCID 53928314 | — |
Reaction Steps
3-(13-Hydroxy-1-tridecynyl)-5-trimethylsilylfuran, prepared as in Example 6, is hydrogenated in ethyl acetate using a poisoned palladium catalyst to give 3-(13-hydroxy-1-tridecenyl)-5-trimethylsilylfuran. Oxidizing by the procedure of Example 7 gives 4-(13-hydroxy-1-tridecenyl)-5-hydroxy-2(5H)-furanone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04957917 |
| Source dataset | uspto-grants-1990_09 |
| ORD ID | ord-46ba467d95af441588e8513b2d2944b4 |
| Source note | uspto-grants-1990_09 |