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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1032528Generated: October 26, 2026

2-(7-nitro-1H-indazol-4-yl)acetonitrile → 2-(3-Methoxy-4-nitrophenyl)acetonitrile

https://huagongshe.com/reaction/1032528

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-(7-nitro-1H-indazol-4-yl)acetonitrileHCID 13629308—
ReactantN,N-Dimethyl-N-[2-(3-methoxy-4-nitrophenyl)ethenyl]amineHCID 54285175—
Product2-(3-Methoxy-4-nitrophenyl)acetonitrileHCID 1362931799.3%

Reaction Steps

19.8 g of N,N-dimethyl-N-[2-(3-methoxy-4nitrophenyl)ethenyl]amine and 30.0 g of hydroxylamineorthosulfonic acid are reacted as described in connection with preparing 2-(7-nitro-1H-indazol-4-yl)acetonitrile, thus obtaining 17.0 g of (3-methoxy-4-nitrophenyl)acetonitrile, mp 85°-86.5° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04958026
Source datasetuspto-grants-1990_09
ORD IDord-5e0df74fa9d84916b8697d0da74d71e9
Source noteuspto-grants-1990_09