Dicyclohexylcarbodiimide → HCID 131716582, compound

HRID 1032621Notes

Reaction equation

HRID 1032621 reaction equation
[CH2:1]([O:9][C:10]1[CH:11]=[C:12]([C:22]([OH:24])=[O:23])[C:13]([C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=2)=[CH:14][CH:15]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].[Cl:25][CH:26]([CH2:41][CH2:42][CH2:43][CH3:44])[CH2:27][C@H:28]([CH3:40])[CH2:29][CH2:30][CH2:31][O:32][C:33]1[CH:38]=[CH:37][C:36](O)=[CH:35][CH:34]=1.C1(N=C=NC2CCCCC2)CCCCC1>ClCCl>[Cl:25][CH:26]([CH2:41][CH2:42][CH2:43][CH3:44])[CH2:27][C@H:28]([CH3:40])[CH2:29][CH2:30][CH2:31][O:32][C:33]1[CH:34]=[CH:35][C:36]([O:23][C:22]([C:12]2[C:13]([C:16]3[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=3)=[CH:14][CH:15]=[C:10]([O:9][CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8])[CH:11]=2)=[O:24])=[CH:37][CH:38]=1

Participants

5

Reactant 3

HCID 10868DicyclohexylcarbodiimideHCID 23162226HCID 23162226, compoundHCID 131716110HCID 131716110, compound

Product 1

HCID 131716582HCID 131716582, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

0.65 g of 4-n-octoxybiphenylcarboxylic acid, 0.60 g of (R)-4-(6'-chloro-4'-methyldecyloxy)phenol, 0.04 g of N,N'-dicyclohexyl carbodiimide and 20 ml of dichloromethane were stirred for 3 hours at room temperature.

Sources & evidence

ORD record
ord-fbd54f8ff4ca45ce8502e7ed695570c0
Source dataset
uspto-grants-1990_09
Patent number
US04959173

Reaction notes

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