Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1032641Generated: October 31, 2026

HCID 13882790, compound → HCID 54694681, compound

https://huagongshe.com/reaction/1032641

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 13882790HCID 13882790—
CatalystPalladiumHCID 23938—
SolventEthyl AcetateHCID 8857—
ProductHCID 54694681HCID 5469468186.4%

Reaction Steps

3-O-Benzyl-2-O-octadecylascorbic acid (2.1 g) was dissolved in ethyl acetate (25 ml), and 5% Pd-C (0.5 g) was added to the solution to conduct catalytic reduction under atmospheric pressure. The catalyst was filtered out, and the filtrate was concentrated under reduced pressure. The reaction product was recrystallized from isopropyl ether-ethyl acetate to give 2-O-octadecylascorbic acid [compound (1-12)](1.5 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04959362
Source datasetuspto-grants-1990_09
ORD IDord-4d2e758d126a47be83928c80ae64da7f
Source noteuspto-grants-1990_09