HCID 19915715, compound → HCID 19915723, compound

HRID 1032675Notes

Reaction equation

HRID 1032675 reaction equation
[N+:1]([C:4]1[CH:25]=[CH:24][C:7]([CH2:8][CH2:9][N:10]([CH2:22][CH3:23])[CH2:11][CH2:12][C:13]2[CH:18]=[CH:17][C:16]([N+:19]([O-])=O)=[CH:15][CH:14]=2)=[CH:6][CH:5]=1)([O-])=O>[H][H].[Pd]>[NH2:19][C:16]1[CH:15]=[CH:14][C:13]([CH2:12][CH2:11][N:10]([CH2:22][CH3:23])[CH2:9][CH2:8][C:7]2[CH:24]=[CH:25][C:4]([NH2:1])=[CH:5][CH:6]=2)=[CH:18][CH:17]=1

Participants

3

Reactant 1

HCID 19915715HCID 19915715, compound

Product 1

HCID 19915723HCID 19915723, compound

Reagents, catalysts & solvents 1

HCID 178506449HCID 178506449, compoundCatalyst

Procedure

N,N-Bis-(4-nitrophenethyl)ethylamine (0.45 g) was reduced using H2 /Pd/C in a similar fashion to Example 23(B) to provide the title compound, yield 0.32 g.

Sources & evidence

ORD record
ord-125c7ebb78f6493fb597cd95ba0bede8
Source dataset
uspto-grants-1990_09
Patent number
US04959366

Reaction notes

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