HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorosulfonyl isocyanate → Benzyl carbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorosulfonyl isocyanate | HCID 70918 | — |
| Reactant | HCID 15682028 | HCID 15682028 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | Benzyl carbamate | HCID 12136 | — |
Reaction Steps
Solution A 1.99 g benzyloxycarbonyl-azetidinon and 1.29 g chlorosulfonyl isocyanate were stirred for 1 hour in 50 ml ethylacetate at 5° C. A solution of (S)-[1-[[chlorosulfonyl)amino]carbonyl]-2-oxo-3-azetidinyl]carbamic acid, phenylmethyl ester was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04959470 |
| Source dataset | uspto-grants-1990_09 |
| ORD ID | ord-609245ca7a3a424dbf262ec125449cb0 |
| Source note | uspto-grants-1990_09 |