HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 4-Decyloxybenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 4-(Decyloxy)benzoic acid | HCID 138527 | — |
| Catalyst | Dimethylformamide | HCID 6228 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | 4-Decyloxybenzoyl chloride | HCID 11779353 | — |
Reaction Steps
A 300 ml two-necked flask equipped with a stirrer and a reflux condenser was charged with 100 ml of carbon tetrachloride, 4.5 ml of thionyl chloride and 11.1 g of 4-n-decyloxybenzoic acid obtained by a conventional method, and heated under reflux together with one drop of dimethylformamide for 4 hours. Then, unreacted thionyl chloride was removed under reduced pressure to obtain 4-decyloxybenzoyl chloride as a colorless liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05308536 |
| Source dataset | uspto-grants-1994_05 |
| ORD ID | ord-de8ea2b0bfca4db4a062d4e0f3d4eec8 |
| Source note | uspto-grants-1994_05 |