HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylene Glycol → HCID 22622966, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylene Glycol | HCID 174 | — |
| Reactant | 4-Hydroxy-3-nitrobenzaldehyde | HCID 18169 | — |
| Reactant | p-Toluenesulfonic acid monohydrate | HCID 521998 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 22622966 | HCID 22622966 | — |
Reaction Steps
A solution of 4-hydroxy-3-nitrobenzaldehyde (known compound, 20.6 g, 124 mmol), benzene (150 ml), ethylene glycol (10.3 ml, 185 mmol) and p-toluenesulfonic acid hydrate (catalytic amount) was refluxed overnight removing the resulting water by azeotropic distillation with benzene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05308840 |
| Source dataset | uspto-grants-1994_05 |
| ORD ID | ord-ba03966fb1ac4db3aba33f1d0f3ef2b8 |
| Source note | uspto-grants-1994_05 |