3-Methyl-4-nitrobenzoic acid → alpha-[p-(dimethylamino)styryl]-N-(2-methyl-4-carboxyphenyl)nitrone

関与物質

反応手順

The general procedure of Example 1 was repeated except that 132.4 g (731 mmols) of 3 -methyl-4-nitrobenzoic acid was used instead of p-nitrobenzoic acid and 118.6 g (677 mmols) of 4-dimethylaminocinnamaldehyde was used instead of 4-diethylaminobenzaldehyde, thereby obtaining 213.8 g (yield 97.4%) of α-[p-(dimethylamino)styryl]-N-(2-methyl-4-carboxyphenyl)nitrone with a purity of 96%. The results of the analyses of the thus obtained compound are shown below.

情報源と証拠