HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiophosgene → HCID 19025453, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiophosgene | HCID 10040 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 19025406 | HCID 19025406 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 19025453 | HCID 19025453 | 101.6% |
Reaction Steps
In a manner similar to Step A of Example 8, the reaction of 3.0 g (0.026 mole) of thiophosgene with 2.6 g (0.013 mole) of 4-diethylamino-2,5-difluoroaniline and 7.2 g (0.052 mole) of potassium carbonate in 100 ml of chloroform and 100 ml of water yielded 3.2 g of 4-diethylamino-2,5-difluorophenyl isothiocyanate. The nmr and ir spectra were consistent with the proposed structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05310724 |
| Source dataset | uspto-grants-1994_05 |
| ORD ID | ord-149563fa953b4068b6a3755786d8ddde |
| Source note | uspto-grants-1994_05 |