HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylhydrazine → HCID 19025429, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylhydrazine | HCID 6061 | — |
| Reactant | HCID 19025396 | HCID 19025396 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19025429 | HCID 19025429 | — |
Reaction Steps
Following procedures similar to those employed in Step A of Example 2, the reaction of 2.2 g (0.0080 mole) of 3,5-dichloro-4-diethylaminophenyl isothiocyanate with 0.37 g (0.0080 mole) of methylhydrazine in 75 ml of ethanol produced a quantitative yield of 4-(3,5-dichloro-4-diethylaminophenyl)-2-methyl-3-thiosemicarbazide. The nmr spectrum was consistent with the proposed structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05310724 |
| Source dataset | uspto-grants-1994_05 |
| ORD ID | ord-624f1d3407774c1ebe40d4d7c76d3e41 |
| Source note | uspto-grants-1994_05 |