HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoic Acid → Benzoic acid--piperidine (1/1)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoic Acid | HCID 243 | — |
| Reactant | Piperidine | HCID 8082 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | Benzoic acid--piperidine (1/1) | HCID 6452737 | 89.9% |
Reaction Steps
To a solution of 12.2 g (0.1 mol) of benzoic acid dissolved in 100 ml of acetone, 8.5 g (0.1 mol) of piperidine was added dropwise. The crystals precipitated were filtered, and then dried, and benzoic acid piperidine salt (molar ratio 1:1) of white crystals was obtained in an amount of 18.6 g (yield 89.9%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05310818 |
| Source dataset | uspto-grants-1994_05 |
| ORD ID | ord-177a0a70932f4672a2af34dca764ac85 |
| Source note | uspto-grants-1994_05 |