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HRID1033380

反应详情

EQUATION

反应方程式

HRID 1033380 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)OC(=O)NC1(C(=O)O)CCCCC1
HCID2794744

1-[(tert-Butoxycarbonyl)amino]cyclohexane-1-carboxylic acid

C12H21NO4

结构：NC1CCc2ccccc2NC1=O
HCID4434433

3-Amino-1,3,4,5-tetrahydro-2H-1-benzazepin-2-one

C10H12N2O

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)NC1(C(=O)NC2CCc3ccccc3NC2=O)CCCCC1
HCID19025470

未命名化合物

PROCEDURE

实验过程

Prepared from 1(t-butoxycarbonylamino)cyclohexanecarboxylic acid and 3-amino-2,3,4,5-tetrahydro-1H-[1]benzazepin-2-one (Example 1, Step A) by the procedure described in Example 25, Step A. 1H NMR (200 MHz, CDCl3): 1.1-2.2 (m,19 H), 2.00 (m,2 H), 2.50 (m,2 H), 4.55 (m,1 H), 6.9-7.2 (m,4 H). FAB-MS: calculated for C22H31N3O4 401; found 402 (M+H,40%).