HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-2-nitrobenzene → 4'-Methyl-2-nitro-1,1'-biphenyl
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-2-nitrobenzene | HCID 11341 | — |
| Reactant | Stannane, trimethyl(4-methylphenyl)- | HCID 617834 | — |
| Product | 4'-Methyl-2-nitro-1,1'-biphenyl | HCID 10443194 | — |
Reaction Steps
Prepared from 4-methylphenyltrimethylstannane (Example 69, Step A) and 2-bromonitrobenzene by the procedure described in Example 69, Step B. 1H NMR (200 MHz,CDCl3): 2.39 (s,3H), 7.23 (m,3H), 7.45 (m,3H), 7.58 (t,7 Hz,1H), 7.80 (d,7 Hz,1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05310737 |
| Source dataset | uspto-grants-1994_05 |
| ORD ID | ord-7dde58cc012747c0854a52129ba78931 |
| Source note | uspto-grants-1994_05 |