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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1033645Generated: October 31, 2026

HCID 15341804, compound → HCID 15341825, compound

https://huagongshe.com/reaction/1033645

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 15341804HCID 15341804—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 15341825HCID 1534182586%

Reaction Steps

1-[2,4-dihydroxy-3-(2-propenyl)benzoyl]pyrrolidine (750 mg) in 2 ml ethanol was hydrogenated at room temperature and 5 psi for three hours using 4% Pd/C as catalyst. The solvent was removed under vacuum and the residue was chromatographed on silica gel using 50/50 ethyl acetate/hexane as eluant to give the product (650 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05310951
Source datasetuspto-grants-1994_05
ORD IDord-ca9468b92a374f6a99fc3bb346ab8b1a
Source noteuspto-grants-1994_05