HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfate → HCID 15341841, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfate | HCID 6497 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 15341840 | HCID 15341840 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 15341841 | HCID 15341841 | — |
Reaction Steps
The compound of Example 63 is methylated (Me2SO4, KOH, THF) under the conditions described in Example 45. Chromatographic purification of the crude product on silica gel (Ethyl acetate/hexane (3:7) as eluant) affords the product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05310951 |
| Source dataset | uspto-grants-1994_05 |
| ORD ID | ord-f53ea2b80dc54b369e37dfa2f3f464fb |
| Source note | uspto-grants-1994_05 |