HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfate → HCID 22399584, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfate | HCID 6497 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 22399587 | HCID 22399587 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 22399584 | HCID 22399584 | — |
Reaction Steps
The compound of Example 73 is treated with dimethyl sulfate and KOH in THF under the conditions described in Example 61. Chromatographic purification of the crude product on silica gel using ethyl acetate/hexane (4:6) as eluant affords the product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05310951 |
| Source dataset | uspto-grants-1994_05 |
| ORD ID | ord-291b490f946b4003a9d975f6392607e4 |
| Source note | uspto-grants-1994_05 |