Hydrazine → 6,11-Dihydro-5H-dibenz[b,e]azepine-6-methanamine

HRID 1033850Notes

Reaction equation

HRID 1033850 reaction equation
C1(=O)[N:5]([CH2:6][CH:7]2[NH:13][C:12]3[CH:14]=[CH:15][CH:16]=[CH:17][C:11]=3[CH2:10][C:9]3[CH:18]=[CH:19][CH:20]=[CH:21][C:8]2=3)C(=O)C2=CC=CC=C12.NN>>[NH2:5][CH2:6][CH:7]1[NH:13][C:12]2[CH:14]=[CH:15][CH:16]=[CH:17][C:11]=2[CH2:10][C:9]2[CH:18]=[CH:19][CH:20]=[CH:21][C:8]1=2

Participants

3

Reactant 2

HCID 9321HydrazineHCID 99466272-[(6,11-Dihydro-5H-dibenzo[b,e]azepin-6-yl)methyl]-1H-isoindole-1,3(2H)-dione

Product 1

HCID 98778946,11-Dihydro-5H-dibenz[b,e]azepine-6-methanamine

Procedure

reacting the 6-(phthalimidomethyl)-6,11-dihydro-5H-dibenz[b,e]azepine with hydrazine in an alkali metal hydroxide to produce 6-aminomethyl-6,11-dihydro-5H-dibenz[b,e]azepine;

Sources & evidence

ORD record
ord-6e3e1c9b05c746b7b159c0976b56c652
Source dataset
uspto-grants-1994_05
Patent number
US05312916

Reaction notes

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