Titanium Tetrachloride → HCID 86746619, compound

Participants

Reaction Steps

A 250 mL Schlenk flask equipped with a magnetic stir bar is charged with titanium tetrakis(di-n-propylamide), 4.49 g (10.0 mmole), and toluene, 100 mL. Titanium tetrachloride, 0.63 g (3.34 mmole), is diluted in toluene, 50 mL, in a 100 mL Schlenk flask then added to the magnetically stirred flask containing titanium tetrakis(di-n-propylamide). The darkly colored solution is refluxed one hour then all volatiles are removed under vacuum. The product, chlorotitanium tris(di-n-propylamide) is used without further purification.

Provenance & Evidence