HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Oxopropanoyl chloride → HCID 86747338, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Oxopropanoyl chloride | HCID 521791 | — |
| Reactant | HCID 86747339 | HCID 86747339 | — |
| Product | HCID 86747338 | HCID 86747338 | — |
Reaction Steps
A method of synthesizing pyruvyl-isoleucine according to the invention the steps of reacting sodium pyruvate with oxalyl chloride to yield pyruvyl chloride, then reacting the pyruvyl chloride with a suspension of isoleucine trimethylsilyl ester hydrochloride to yield pyruvyl-isoleucine trimethylsilyl ester and then subjecting the pyruvyl-isoleucine trimethylsilyl ester to hydrolysis to yield pyruvyl-isoleucine. The pyruvyl-isoleucine synthesized via the method set forth above serves as a pyruvyl-amino acid pyruvate precursor.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05312985 |
| Source dataset | uspto-grants-1994_05 |
| ORD ID | ord-3eb415ef4ab646deb535e23a897ef69d |
| Source note | uspto-grants-1994_05 |