HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Oxopropanoyl chloride → HCID 67575675, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Oxopropanoyl chloride | HCID 521791 | — |
| Reactant | HCID 67575593 | HCID 67575593 | — |
| Product | HCID 67575675 | HCID 67575675 | — |
Reaction Steps
A method of synthesizing pyruvyl-phenylalanine according to the invention comprises the steps of reacting sodium pyruvate with oxalyl chloride to yield pyruvyl chloride, then reacting pyruvyl chloride with a suspension of phenylalanine trimethylsilyl ester hydrochloride to yield pyruvyl-phenylalanine trimethylsilyl ester and then subjecting the pyruvyl-phenylalanine trimethylsilyl ester to hydrolysis to yield pyruvyl-phenylalanine. The pyruvyl-phenylalanine synthesized via the route set forth above serves as a pyruvyl-amino acid pyruvate precursor.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05312985 |
| Source dataset | uspto-grants-1994_05 |
| ORD ID | ord-8d1ae7911c7f4c90861171c189cbff2f |
| Source note | uspto-grants-1994_05 |