HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1034056Generated: October 31, 2026
Carbon tetrabromide → 1-(1-Bromoethyl)-3-isobutylbenzene
https://huagongshe.com/reaction/1034056
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Carbon tetrabromide | HCID 11205 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | 1-(3-Isobutylphenyl)ethanol | HCID 19024774 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 1-(1-Bromoethyl)-3-isobutylbenzene | HCID 19024846 | 100.1% |
Reaction Steps
A mixture of 1-(3-isobutylphenyl)ethanol (1.1 g), triphenylphosphine (3.24 g) and carbon tetrabromide (4.09 g) in ether (20 ml) was stirred at 25° C. for 1 hour. The precipitates were filtered off, and the liltrate was evaporated to give 1-(1-bromoethyl)-3-isobutylbenzene (1.49 g) as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05312829 |
|---|
| Source dataset | uspto-grants-1994_05 |
|---|
| ORD ID | ord-e4854311a4904498805cb8fa114ada91 |
|---|
| Source note | uspto-grants-1994_05 |
|---|
