HCID 178445573, compound → HCID 178447704, compound

HRID 1034126Notes

Reaction equation

HRID 1034126 reaction equation
[NH2:1][C:2]1[N:6]=[C:5]([S:7][CH2:8][CH2:9][CH2:10][S:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16])[NH:4][N:3]=1.C(SCCSCCSC1N=C2N(N=1)[C:36]([OH:39])=[CH:35][C:34]([CH3:40])=N2)CCCCC>>[CH2:12]([S:11][CH2:10][CH2:9][CH2:8][S:7][C:5]1[N:6]=[C:2]2[N:3]([N:4]=1)[C:36]([OH:39])=[CH:35][C:34]([CH3:40])=[N:1]2)[CH2:13][CH2:14][CH2:15][CH3:16]

Participants

3

Reactant 2

HCID 178445573HCID 178445573, compoundHCID 1784477053-Amino-5-[3-(pentylthio)propylthio]-1,2,4-triazole

Product 1

HCID 178447704HCID 178447704, compound

Procedure

Compound 18 was prepared from Compound 9, using a procedure analogous to that described previously for Compound 20. The crude product was recrystallized from ethyl acetate to give a 24% yield of white solid, m.p. 121°-123° C. Analysis: Calculated for C14H22N4OS2 : C, 51.50; H, 6.79; N, 17.16. Found: C, 51.30; H, 6.69; N, 16.97.

Workup

  1. customThe crude product was recrystallized from ethyl acetate

Sources & evidence

ORD record
ord-2e12c1c6d2b74d8095163b2fab21694f
Source dataset
uspto-grants-1994_05
Patent number
US05314790

Reaction notes

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