Methyl iodide → HCID 85648911, compound

HRID 1034203Notes

Reaction equation

HRID 1034203 reaction equation
[CH3:1][O:2][N:3]=[C:4]([C:7]1[CH:8]=[N:9][CH:10]=[CH:11][CH:12]=1)[C:5]#[N:6].[CH3:13][I:14]>CO>[I-:14].[CH3:1][O:2][N:3]=[C:4]([C:7]1[CH:8]=[N+:9]([CH3:13])[CH:10]=[CH:11][CH:12]=1)[C:5]#[N:6]

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 53756267HCID 53756267, compound

Product 1

HCID 85648911HCID 85648911, compoundYield 100%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

α-(Methoxyimino)-α-(pyridin-3-yl) acetonitrile (D2) (0.155 g, 0.00096 mol) was heated under reflux with methyl iodide (5 ml) in methanol (5 ml) for 60 h. The mixture was evaporated to dryness to give the title compound (D3) (0.3 g, 100%) which was used without further purification.

Workup

  1. customThe mixture was evaporated to dryness

Sources & evidence

ORD record
ord-d7fdbe1e69db41259351ddc1a1ad943a
Source dataset
uspto-grants-1994_05
Patent number
US05314901

Reaction notes

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