Hydroxyamine hydrochloride → HCID 131717849, compound

Participants

Reaction Steps

To the title compound of Example J (21.6 g, 0.085 mol) in pyridine (150 ml) was added hydroxylamine hydrochloride (10.6 g, 0.17 mol) and the solution was stirred for 5 days. The solvent was removed in vacuo to give an orange oil which as chromatographed on silica gel eluting with 2% EtOH/CH2Cl2 to give the title compound (13.67 g, 59%) as an oil. Calculated C13H22N2O4 1/2H2O: C, 55.90; H, 8.30; N, 10.02 Found: C, 55.99; H, 8.38; N, 10.00. MS calcd for C13H22N2O4 270, found 270.

Provenance & Evidence