HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 4-(hydroxyimino)-5-oxo-1-phenyl-3-pyrrolidineacetate → Ethyl 4-amino-5-oxo-1-phenyl-3-pyrrolidineacetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 4-(hydroxyimino)-5-oxo-1-phenyl-3-pyrrolidineacetate | HCID 86746704 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Ethyl 4-amino-5-oxo-1-phenyl-3-pyrrolidineacetate | HCID 53812745 | — |
Reaction Steps
A solution of the product of example 63 in EtOH is hydrogenated with 10% palladium on carbon at 60 psi at 60° C. Filtration and purification of the product on silica gel affords the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05314886 |
| Source dataset | uspto-grants-1994_05 |
| ORD ID | ord-f6428ceea59541f69d5d9979113c4bc9 |
| Source note | uspto-grants-1994_05 |