HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Dithionite → Bis(2-(methylcarbamoyl)cyclopenten-1-yl) disulfide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Dithionite | HCID 24489 | — |
| Reactant | 2-Methyl-4,5-trimethylene-4-isothiazolin-3-one | HCID 158190 | — |
| Solvent | Water | HCID 962 | — |
| Product | Bis(2-(methylcarbamoyl)cyclopenten-1-yl) disulfide | HCID 19023919 | — |
Reaction Steps
2-methyl-4,5-trimethylene-4-isothiazolin-3-one (1 part) was stirred in distilled water (25 parts) at 20°-25° C. Sodium hydrosulphite (2×0.2 parts) was added in two portions over 30 minutes. Analysis by HPLC indicated the formation of two products.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05315009 |
| Source dataset | uspto-grants-1994_05 |
| ORD ID | ord-efb40daf291442409126f18f2e75069a |
| Source note | uspto-grants-1994_05 |