HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 10-Methylacridan-9-carboxylic acid chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 10-Methylacridan-9-carboxylic acid | HCID 10399341 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 10-Methylacridan-9-carboxylic acid chloride | HCID 54520729 | — |
Reaction Steps
A solution of 0.35 parts of 10-methylacridan-9-carboxylic acid (77) in 20 mL dichloromethane and 1.1 parts of thionyl chloride is treated as described in Example I, to give 10-Methylacridan-9-carboxylic acid chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546150B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-1a33e3f3ac00447ea28dd7a464226029 |
| Source note | uspto-grants-2013_10 |