3-Cyanophenol → HCID 68584125, compound
Reaction equation
[OH:1][C:2]1[CH:3]=[C:4]([CH:7]=[CH:8][CH:9]=1)[C:5]#[N:6].F[C:11]1[CH:16]=[C:15]([CH3:17])[CH:14]=[CH:13][N:12]=1>>[CH3:17][C:15]1[CH:14]=[CH:13][N:12]=[C:11]([O:1][C:2]2[CH:3]=[C:4]([CH:7]=[CH:8][CH:9]=2)[C:5]#[N:6])[CH:16]=1Participants
3
Procedure
3-Hydroxy-benzonitrile was reacted with 2-fluoro-4-methylpyridine according to the method of Example 78A to provide the title compound. MS (DCI/NH3) m/z 211 (M+1)+.
Sources & evidence
- ORD record
- ord-08177f4d366e4aceb7789acbddcb7468
- Source dataset
- uspto-grants-2013_10
- Patent number
- US08546374B2
Reaction notes
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