Thionyl Chloride → HCID 86082255, compound

HRID 1035022Notes

Reaction equation

[N:1]1[CH:6]=[CH:5][C:4]([C:7]2[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=2[CH2:13]O)=[CH:3][CH:2]=1.S(Cl)(Cl)=O.[N-:19]=[N+:20]=[N-:21].[Na+]>>[N:19]([CH2:13][C:8]1[CH:9]=[CH:10][CH:11]=[CH:12][C:7]=1[C:4]1[CH:5]=[CH:6][N:1]=[CH:2][CH:3]=1)=[N+:20]=[N-:21]

Participants

Reactant 3

HCID 24386Thionyl Chloride

HCID 33557Sodium Azide

HCID 14955123(2-(Pyridin-4-yl)phenyl)methanol

Product 1

HCID 86082255HCID 86082255, compound

Procedure

The product of Example 120A, thionyl chloride and sodium azide were processed according to the method of Example 115A to provide the product. MS (ESI+) m/z 211 (M+H)+.

Workup

customto provide the product

Sources & evidence

ORD record: ord-fae13631434c4ec5857983106a001b11
Source dataset: uspto-grants-2013_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08546374B2

Reaction notes

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