3-(Azidomethyl)-2-ethylpyridine → (2-Ethylpyridin-3-yl)methanamine

HRID 1035026Notes

Reaction equation

HRID 1035026 reaction equation
[N:1]([CH2:4][C:5]1[C:6]([CH2:11][CH3:12])=[N:7][CH:8]=[CH:9][CH:10]=1)=[N+]=[N-]>[Pd]>[CH2:11]([C:6]1[C:5]([CH2:4][NH2:1])=[CH:10][CH:9]=[CH:8][N:7]=1)[CH3:12]

Participants

3

Reactant 1

HCID 860822563-(Azidomethyl)-2-ethylpyridine

Product 1

HCID 55267213(2-Ethylpyridin-3-yl)methanamine

Reagents, catalysts & solvents 1

HCID 23938PalladiumCatalyst

Procedure

The product of Example 124B and Pd/C were processed according to the method of Example 115B to provide the product. MS (ESI+) m/z 137 (M+H)+.

Workup

  1. customto provide the product

Sources & evidence

ORD record
ord-4203f3ced96048b29216f8e41f03fd04
Source dataset
uspto-grants-2013_10
Patent number
US08546374B2

Reaction notes

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