HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 3-(Azidomethyl)-2-chloro-5-fluoropyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | (2-Chloro-5-fluoropyridin-3-yl)methanol | HCID 24229204 | — |
| Product | 3-(Azidomethyl)-2-chloro-5-fluoropyridine | HCID 86082262 | — |
Reaction Steps
(2-chloro-5-fluoro-pyridin-3-yl)-methanol, thionyl chloride and sodium azide were processed according to the method of Example 115A to provide the product. MS (ESI+) m/z 187 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546374B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-0a71683e5ae641dfb82602c4da1eee96 |
| Source note | uspto-grants-2013_10 |